CHEN 4860 Laboratory Manual- Fall 2011

1. Batch Assignment Fall'11 (use 0.20 M NaOH, not 0.25)
2. Flow Reactors (CSTR) Work with instructor to develop methods and do experiment.  Handout for analysis given in lab period.
3. For Prelab- tace piping and instrumentation system- prepare for questions about unit.
4. Primer on Visible and UV Spectroscopy
5. Ocean Optics pectrometer dip-probe manual
6. How Spectrophotometers work
7. How CCD detectors work
8. Fogler Text- chapters on CSTRs
9. Cosaro, G Journal of Chemical Education, 41,48, 1964
10. Andres DP and LR Hile, Chemical Engineering Education, Winter 1976, p18
11. Lalane JR, Determination of pKa of phenolphthalien and it's discloration rate, Journal of Chemical Education, 1971, 48-4 266-268
12. Nicolson L, Kinetics of the fading of phenolphthalien in alkaline solution, Journal of Chemical Education, 1989, 66-9 725-728

1. Assignment Spring08
2. Lecture slides
3. DO. meter manual
4. Saturated O₂ vs T&P  table
5. Impeller Dimensions
6. Bioreactor Data Acquisition Program
7. Geankoplis section 3.4
8. Biochemical Engineering Text (Bailey & Ollis, etc)
9. Perry's Handbook

1. Ion Exchange Proceedure and Analysis Fall 2011
2. Ion exchange archive (with resin data)
3. Ion-x info from Perrys 6th edition
4. Ocean Optics Spectrometer manual
5. Geankoplis 4^th ed. chapter 12

References:

1. Distillation Assignment, Fall 2011 as of 8/25/11
2. Apparatus Detail Photos
3. VLE Data & McCabe-Thiele
4. Calibration Curves
5. Alcohol Physical Properties
6. Seader & Henley, Separation Process Principles, 2nd ed., Ch. 7
7. Geankoplis, 4th ed., Chapter 11

* New photos and directions reflecting improvements to the distillation column
for Fall of 2010 will be posted soon.

1. Assignment, Fall'11
2. Note on tray thermocouples
3. Geankoplis 4^th ed. Chapter 9
4. Geankoplis 4^th ed., sect. 6.2C; 6.5C

Popcorn Data .dx6 file- May or may not load from web in dx.7

mans486/DOE/popcorn.dx6

The Evaporator projects for Fall 2010 may vary from group to group, and will go beyond what you may have done in 3820. The assignments will reflect ongoing modification to the unit as the semester progresses.  You will help test equipment changes (addition of pumps and valves) and help write operating procedures. By the end of the semester we hope to be running in double effect mode, concentrating a salt solution.  The first lab assignment will be posted soon.

Process Flow Sheet

Video1  Video2

Feed water flow meter calibration

Additional data and specifications

Table of external heat transfer coefficients

References:

ref #1- Geankopolis, 4th ed. Chapter 8

ref# 2- McCabe, Smith and Harriot- Chapter 16

ref #3- Chemical Equipment CD from Felder & Rouseau