Diamond Synthesis in Perspective

 

James Sung

 

China Grinding Wheel Corporation, Taipei, Taiwan, ROC

Taipei University of Technology, Taipei, Taiwan, ROC

 
Abstract

 

Diamond may be converted directly from a non-diamond carbon source in microseconds by a displacive movement of atoms without diffusion, or synthesized catalytically in minutes by reconstructive means with the transport of atoms.  The diamond formation pressure and temperature are dependent on the time scale and the structure of the carbon source.  The instant conversion may occur with zero-dimensional carbon (point-like sp0 atoms) by PVD, one-dimensional carbon (line-like sp1 chains) by dynamite detonation, or two-dimensional carbon (plane-like sp2 surface) by shock wave compaction. The timely synthesis may proceed with two-dimensional (sp2) graphite (e.g., by puckering recrystallized flakes in a molten catalyst, or with three-dimensional (sp3) diamond-like molecules such as solute atoms in a molten catalyst (e.g., by temperature gradient method), or caged atoms in methane molecules (e.g., by CVD).

The approximate activation energies (E) for the major diamond synthesis methods may be estimated from their reaction routes.  The threshold pressure and temperature for each of these synthesis routine may be calculated based on the estimated activation energy.  The results are summarized in the following table.

 

C Source        State      Method                     Route              Time                E(eV)            P(Gpa)       T(oC)

Plasma            sp0          PVD                          Direct             Instant             0.33              16              3500

Dynamite        sp1          Explosion                 Direct             Instant             0.25              12              2700

Graphite         sp2          Shock Wave            Direct             Instant             0.17              8.1             1800

Graphite         sp2          Puckering               Catalytic         Timely             0.13              6.2             1250

Solute              sp3          Precipitation           Catalytic         Timely             0.13              6.2             1250

Methane          sp3          Adjoining                 Catalytic         Timely             0.09              4.3             800 

 

Keywords: Diamond Synthesis, Diamond Catalyst, PVD Diamond, CVD Diamond